12. Evaporation, condensation,
collecting -Distillation of coloured water
This
experiment requires adult supervision
In the previous
experiment the water completely evaporated. Now water vapour will be cooled
and transferred into an second container.
What
to do
1. Distillation on an electric
hotplate in a demo experiment (Photo
1, 3, 4) with 20 ml.
2. Distillation
in a student experiment with 3 ampoules (Photo 5) with 2 ml.
Material
Tray, 2 infusion
bottles 50 ml with stopper, 4 ampoules (5ml) high with stopper, 2 plastic
pipette tips, 50 cm infusion tube, toilette paper, cotton wool, scissors, insulated
copper wire, 2 boiling aids (Photo 2: coiled
copper wire), electric hotplate, digital thermometer,
water coloured by Cola or stale Cola.
Experiment
1
1. Connect a 50-ml infusion bottle
and an ampoule with an insulated copper wire.
2. Pierce the stopper of the infusion
bottle twice: One pipette tip from downside, a second one from upside.
3. Add 20 ml of water, some Cola
and a boiling aid to the bottle, close it, place it on the electric hotplate,
start heating.
4. Press 20 cm of infusion tube over
the thin end of the pipette tip.
5. Fill the second infusion bottle
with cooling water. Dip the ampoule into it (Photo
1).
6. Fix the free end of the tube in
the upper part of the ampoule.
7.
Press the sensor of the digital thermometer through the 2. pipette tip.
9. Watch the increase of temperature,
changes in the tube and in the ampoule (Photo
3 and 4).
10 Stop the experiment when 2 ml
of liquid have collected in the ampoule.
Observation
The
coloured water boils, colourless drops appear inside the tube and drop into
the ampoule.
Explanation
Water evaporates, the substances
dissolved do not. The vapour condenses during cooling.
Experiment
2 (Photo 5)
The electric hotplate is replaced
by a burner made from an ampoule and the infusion bottle by another ampoule.
Observation
and Explanation
Like
in experiment 1. .